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Application in the Synthesis of Ligands for Asymmetric Catalysis

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Asymmetric synthesis | Enantioselective Synthesis | B Cell

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Bin Mao was born in Zhuji, Zhejiang, China, in 1983. He received his B.S. in chemistry in 2005 and M.S. in biochemistry in 2009 from Lanzhou University under the direction of Prof. Rui Wang. After graduate work at the University of Groningen in the laboratories of Ben L. Feringa and an postdoctoral fellowship at Memorial Sloan-Kettering Cancer Center with Derek Tan, he took a position at the Zhejiang University of Technology in 2016. He is currently assistant professor at the Collaborative Innovation Center of Yangtze River Delta Region Green Pharmaceuticals. His research interests lie in the development of new methodology toward the asymmetric synthesis of biologically active products as well as novel molecular probes applied in the field of chemical biology.

Asymmetric Synthesis | SpringerLink

A Novel Asymmetric Synthesis of Unsaturated Aromatic 1,2-Amino Alcohols

Ben L. Feringa obtained his Ph.D. degree in 1978 at the University of Groningen in The Netherlands under the guidance of Prof. Hans Wynberg. After working as a research scientist at Shell, he was appointed full professor at the University of Groningen in 1988 and named the distinguished Jacobus H. van’t Hoff Professor of Molecular Sciences in 2004. He was elected a foreign honorary member of the American Academy of Arts and Sciences and a member of the Royal Netherlands Academy of Sciences. His research interests include stereochemistry, organic synthesis, asymmetric catalysis, molecular switches and motors, self-assembly, and nanosystems.

The development of a scalable asymmetric route to a new calcitonin gene-related peptide (CGRP) receptor antagonist is described. The synthesis of the two key fragments was redefined, and the intermediates were accessed through novel chemistry. Chiral lactam 2 was prepared by an enzyme mediated dynamic kinetic transamination which simultaneously set two stereocenters. Enzyme evolution resulted in an optimized transaminase providing the desired configuration in >60:1 /. The final chiral center was set via a crystallization induced diastereomeric transformation. The asymmetric spirocyclization to form the second fragment, chiral spiro acid intermediate 3, was catalyzed by a novel doubly quaternized phase transfer catalyst and provided optically pure material on isolation. With the two fragments in hand, development of their final union by amide bond formation and subsequent direct isolation is described. The described chemistry has been used to deliver over 100 kg of our desired target, ubrogepant.

Dynamic kinetic resolution in asymmetric synthesis - …

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AB - An efficient asymmetric synthesis of (+)-tetrahydropseudodistomin is described. The important synthetic features include a Maruoka asymmetric allylation and a Sharpless asymmetric dihydroxylation as key steps for the generation of chirality at C-2, -4, and -5 of the trisubstituted piperidine ring.

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  • Catalytic Asymmetric Synthesis - Nobel Prize

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  • Asymmetric Synthesis - Garry Procter - Oxford …

    Enantioselective synthesis, also called asymmetric synthesis, is a form of chemical synthesis

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14/01/2018 · Looking for asymmetric synthesis

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