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ORGANOMETALLICS IN SYNTHESIS A MANUAL

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Tables of 1H and 13C NMR resonances for common organic contaminants are reported in 12 different deuterated organic solvents frequently used to study organometallic systems. This manuscript catalogs the chemical shifts for nearly 60 gases and organic compounds which are commonly used as reagents or internal standards or are found as products in organometallic reactions.

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Tables of 1H and 13C NMR chemical shifts have been compiled for common organic compounds often used as reagents or found as products or contaminants in deuterated organic solvents. Building upon the work of Gottlieb, Kotlyar, and Nudelman in the signals for common impurities are now reported in additional NMR solvents (tetrahydrofuran-8, toluene-8, dichloromethane-2, chlorobenzene-5, and 2,2,2-trifluoroethanol-3) which are frequently used in organometallic laboratories. Chemical shifts for other organics which are often used as reagents or internal standards or are found as products in organometallic chemistry are also reported for all the listed solvents.

Organometallics In Synthesis A Manual Pdf

ORGANOMETALLICS IN SYNTHESIS THIRD MANUAL

An improved method for the preparation of graphene oxide (GO) is described. Currently, Hummers’ method (KMnO4, NaNO3, H2SO4) is the most common method used for preparing graphene oxide. We have found that excluding the NaNO3, increasing the amount of KMnO4, and performing the reaction in a 9:1 mixture of H2SO4/H3PO4 improves the efficiency of the oxidation process. This improved method provides a greater amount of hydrophilic oxidized graphene material as compared to Hummers’ method or Hummers’ method with additional KMnO4. Moreover, even though the GO produced by our method is more oxidized than that prepared by Hummers’ method, when both are reduced in the same chamber with hydrazine, chemically converted graphene (CCG) produced from this new method is equivalent in its electrical conductivity. In contrast to Hummers’ method, the new method does not generate toxic gas and the temperature is easily controlled. This improved synthesis of GO may be important for large-scale production of GO as well as the construction of devices composed of the subsequent CCG.

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