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D-Glucaric acid, compd. with (αS)-α-methylbenzeneethanamine (1:2)

N,N,N-trimethyl-4-[(4,7,7-trimethyl-3-oxobicyclo[2.2.1]hept-2-ylidene)methyl]benzenaminim, methyl

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2-Chlorotoluene For Synthesis | VWR

When the amount of catalyst is close to 1.5 mL, yield increases more slowly, taking into account the cost of the catalyst, and the product cost etc.,

The choice of 1.25 mL was the best dosage.

1.2 effect of the dosage of KMnO4

This column experiments of A-1 1.25 mL, p-chlorotoluene 6 mL, H2O 216 mL, KMnO4 = 15.805 g, 17.284 g, 20.545 g, 23.706 G.

o-Chlorotoluene and p-Chlorotoluene could be produced through the following synthetic routes

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4-Chlorotoluene | Sigma-Aldrich

Pursuant to subsection 71(3) of the Act, every person to whom this notice applies shall comply with this notice within the time specified in the notice. The time specified in this notice is July 17, 2017, 3 p.m., Eastern Daylight Saving Time. Any person making a written request pursuant to subsection 71(4) of the Act should include the name of the party requiring an extension, the Chemical Abstracts Service Registry Number (CAS RN) of the substances for which the person will provide information, as well as the reason of the extension request.

At about 80 ℃ into 6 mL p-chlorotoluene, temperature 92 ~ 96 ℃, the Potassium Permanganate fade as a reference.

1.3 effect of reaction time

With the increase of the content of the Potassium Permanganate yield increased gradually, but 20.545 g yield increased speed slow, in order to reduce the cost as much as possible, Potassium Permanganate cannot consume too much, so the same reaction conditions, Potassium Permanganate dosage is 20.545 G.

1.4 effect of reaction temperature

The column experiment Potassium Permanganate 20.545 g, p-chlorotoluene 6mL, catalyst A-1 1.25 mL, water was 216 mL.

Search results for 4-Chlorotoluene at Sigma-Aldrich

Therefore, the effects of amount of catalyst on the reaction.

This column is about 18.970 g reaction Potassium Permanganate, p-chlorotoluene 6 mL, H2O216 mL, catalyst A-1, catalyst A-1, the Potassium Permanganate, water with three neck bottle, at about 80 ℃ into p-chlorotoluene, temperature 90 ℃, reaction at 2 h for reference.

Without catalyst reaction is extremely slow, with the increased dosage of catalyst A-1, 4-chlorobenzoic acid yield was also increased to maximum yield is 1.5, catalyst mL.

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