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American Journal of Organic Chemistry

p-ISSN: 2163-1271 e-ISSN: 2163-1301

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 Keywords:    Quinoxaline, Phenol, 1,2-Diamine, Α-Diketone, Green Chemistry

A new method was developed for the synthesis of quinoxalines. This method employs -arylenamines and TMSN3 as the starting materials and implements two oxidative C–N bond-forming processes in a tandem pattern by using (diacetoxyiodo)benzene as the common oxidant. The present reaction conditions are mild and simple and thus are useful in practical synthesis.

JO - Journal of Organic Chemistry

General experimental procedures, characterization data for the substrates and products, 1H NMR and 13C NMR spectra of the substrates and products ()

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T2 - Journal of Organic Chemistry

The first total synthesis of the biologically significant bis-indole alkaloid dragmacidin D (5) has been achieved. Thermal and electronic modulation provides the key for a series of palladium-catalyzed Suzuki cross-coupling reactions that furnished the core structure of the complex guanidine- and aminoimidazole-containing dragmacidins. Following this crucial sequence, a succession of meticulously controlled final events was developed leading to the completion of the natural product.

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    2012; 2(4): 97-104

  • Crystallographic data for compound 2f ()

    Abstract

  • 1155 Sixteenth Street N.W.Washington, DC 20036

    ChemSynthesis - Chemical Database

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1155 Sixteenth Street N.W.Washington, DC 20036

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Scott E. Allen was born in 1984 in Kutztown, Pennsylvania. He received his B.S. in chemistry from Penn State University, where he performed undergraduate research with Dr. Xumu Zhang. He then joined the laboratory of Dr. Marisa C. Kozlowski at the University of Pennsylvania, where his research focused on computational organic chemistry studies of N-heterocyclic carbene-catalyzed reactions in collaboration with Dr. Jeffery Bode at the ETH. Upon completion of his Ph.D. in early 2013, Scott joined the laboratory of Dr. Albert Bowers at the UNC Eshelman School of Pharmacy as a postdoctoral associate.

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