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Synthesis and Analysis of a Coordination Compound.

Study Chemistry 212 Synthesis of a Coordination Compound lab report notes.

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Synthesis And Analysis Of Coordination Compounds ..

Abstract:
The current interest of our research group is largely focused on the development and understanding of precipitated crystalline organometallic compounds. We are placing a strong emphasis in the study of the synthetic procedures, the morphology, and on the structural determination of such compounds. Special importance is engaged in the preparation coordination polymers crystallized from solutions of supercritical CO2, (scCO2), where the use of a co-solvent is occasionally employed depending on reagents solubility [1-3]. The correct selection of experimental conditions in the scCO2 reactive crystallization technique, allows a precipitation known from other methodologies, as well as new crystalline phases. This procedure leads to the crystallization of stable hierarchical nanoestructures involving micro and mesoporosity. As the preparation of the crystalline materials is carried out in scCO2, these obtained with microporous structures were recovered activated, i.e., with open volume, since the removal of any guest molecules from the framework is carried out by simple depressurization. This method is expected to have many potential applications in the development of green crystallization techniques for coordination polymers synthesis.

Synthesis and Analysis of a Coordination Compound

Biography:
Dr. Naoufel Khemiri is an Assistant Professor at El Manar Preparatory Engineering Institute in Tunisia. He obtained his Ph.D thesis in “Condensed Matter Physics” from the Faculty of Sciences of Tunis (FST), University of Tunis El Manar, Tunisia in 2012. He is now member of Photovoltaic and Semiconductor Materials Laboratory (ENIT, Tunis, Tunisia). He works mainly on the synthesis and the characterization of ternary and quaternary compounds (CuInS2, Zn(S,O), SnSb4S7, Cu2ZnSnS4 and Cu2ZnxFe1-xSnS4) for opto-electronic and solar cell applications. He published more than 20 papers in International Journals with impact factor and participated in several international conferences in materials science.

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08/05/2014 · Synthesis and analysis of a coordination compound of copper lab >>> click here Examples of a level psychology essays

An undergraduate chemistry laboratory project involving the synthesis of [Ag(NH3)2]2SO4 and Cu(NH3)4SO4 from the simple sulfate salts is described. Characterization of the stoichiometry of the complexes is accomplished by gravimetric and volumetric analysis. Silver is precipitated as the chloride and copper is precipitated as the hydroxide and converted to the oxide before weighing. The ammonia content of each complex is determined with a back titration using dilute nitric acid and sodium hydroxide. Typical student work gives results for the stoichiometry of the complexes within 1-5% of the theoretical values. The project provides a convenient preparation of two compounds whose identity and formula will not be obvious to the student. The analytical procedures illustrate the fundamentals of gravimetric and volumetric analysis and some basic characteristics of simple coordination complexes. The analytical data allow the student to determine the identity of each product by determining its empirical formula.

Biography:
Rajiv Prakash is professor and coordinator of the School of Materials Science and Technology, Indian Institute of Technology (Banaras Hindu University), Varanasi, India. He has been recipients of Young Scientist (Council of Science and Technology), Young Engineer Awards (INAE) of India and Materials Society Medal Award of India. His current research interests include synthesis of morphology controlled organic conducting polymers, nanocomposites, fabrication and characterization of organic electronic devices and sensors/biosensors. He is having more than 150 publications in international journals of repute and 17 patents in his credit. He is in Editorial Board of several National and International Journals. He is member of various national committees including DST-TIFAC for India Vision 2035 and MHRD “IMPRINT” program.

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Books Lab Report Gravimetric Analysis Of Calcium Chloride Pdf synthesis and analysis of a coordination compound of copper - synthesis and analysis of a

Biography:
Dr. Naoufel Khemiri is an Assistant Professor at El Manar Preparatory Engineering Institute in Tunisia. He obtained his Ph.D thesis in “Condensed Matter Physics” from the Faculty of Sciences of Tunis (FST), University of Tunis El Manar, Tunisia in 2012. He is now member of Photovoltaic and Semiconductor Materials Laboratory (ENIT, Tunis, Tunisia). He works mainly on the synthesis and the characterization of ternary and quaternary compounds (CuInS2, Zn(S,O), SnSb4S7, Cu2ZnSnS4 and Cu2ZnxFe1-xSnS4) for opto-electronic and solar cell applications. He published more than 20 papers in International Journals with impact factor and participated in several international conferences in materials science.

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