T1 - Asymmetric synthesis of ageliferin
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Mathieu Bosch graduated from the University of Houston in 2013 with a B.S. in chemistry, and immediately thereafter joined Dr. Hong-Cai Zhou’s group as a Ph.D. student at Texas A&M University. His research focuses on pore engineering in MOFs and porous polymers, and the development of MOF synthesis and postsynthetic modification techniques.
"The high potency of pateamine A against a wide array of tumor cell lines, along with the fact that it induces stress granule formation," suggests that the natural product and its analogs, such as a more synthetically accessible derivative, desmethyldesaminopateamine A (
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Topics of interest include, but are not limited to: hardwaresynthesis and optimization; software synthesis; hardware/softwareco-synthesis; power and timing analysis; testing, validation andverification; synthesis for reconfigurable architectures; hardwarecompilation for domain-specific languages; designexperiences. Submissions on modeling, analysis and synthesis foremerging technologies and platforms are particularly encouraged.
: Synthesis gas, a mixture of hydrogen, carbon monoxide, and a small amount of carbon dioxide, is created by reacting natural gas with high-temperature steam. The carbon monoxide is reacted with water to produce additional hydrogen. This method is the cheapest, most efficient, and most common. Natural gas reforming using steam accounts for the majority of hydrogen produced in the United States annually.
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Shuai Yuan graduated from Shandong University in 2013, where he studied the design and synthesis of luminescent MOFs. He became a Ph.D. student in Dr. Hong-Cai Zhou’s group at Texas A&M University in 2013, and he focuses his research on the design and synthesis of metal–organic frameworks for gas storage, gas separation and catalysis.
AB - We describe herein an asymmetric synthesis of ageliferin. A Mn(III)-mediated oxidative radical cyclization reaction was used as the key step to construct the core skeleton of this pyrrole-imidazole dimer. This approach resembles the biogenic [4 + 2] dimerization in an intramolecular fashion.
We describe herein an asymmetric synthesis of ageliferin
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N2 - We describe herein an asymmetric synthesis of ageliferin. A Mn(III)-mediated oxidative radical cyclization reaction was used as the key step to construct the core skeleton of this pyrrole-imidazole dimer. This approach resembles the biogenic [4 + 2] dimerization in an intramolecular fashion.
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A synthesis gas can also be created by reacting coal or biomass with high-temperature steam and oxygen in a pressurized gasifier, which is converted into gaseous components—a process called gasification. The resulting synthesis gas contains hydrogen and carbon monoxide, which is reacted with steam to separate the hydrogen.
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William Rutledge graduated from Millersville University in 2014, after researching iridium N-heterocyclic carbene-based transfer hydrogenation catalysts, and became a member of Dr. Hong-Cai Zhou’s group at Texas A&M University as a Ph.D. student in 2015. His research is on the synthesis of new MOF materials specialized towards clean energy technologies.
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Hong-Cai “Joe” Zhou graduated from Texas A&M University with his Ph.D. in 2000 under the supervision of Prof. F. A. Cotton. He then completed postdoctoral research with Prof. R. H. Holm at Harvard University in 2002, and became a faculty member at Miami University, Oxford. In 2008, he became a full professor at Texas A&M University, a Davidson Professor of Science in 2014, and a Robert A. Welch Chair in Chemistry in 2015. His research focuses on synthetic methods to obtain extremely stable framework and other porous materials with interesting and useful catalytic or clean-energy related properties.
Stepwise Synthesis of Metal–Organic Frameworks - …
Metal–organic frameworks (MOFs) are a category of porous materials that offer unparalleled control over their surface areas (demonstrated as higher than for any other material), pore characteristics, and functionalization. This allows them to be customized for exceptional performance in a wide variety of applications, most commonly including gas storage and separation, drug delivery, luminescence, or heterogeneous catalysis. In order to optimize biomimicry, controlled separations and storage of small molecules, and detailed testing of structure–property relationships, one major goal of MOF research is “rational design” or “pore engineering”, or precise control of the placement of multiple functional groups in pores of chosen sizes and shapes. MOF crystal growth can be controlled through judicious design of stepwise synthetic routes, which can also allow functionalization of MOFs in ways that were previously synthetically inaccessible. Organic chemists have developed a library of powerful techniques over the last century, allowing the total synthesis and detailed customization of complex molecules.
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